2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

Base Information

Chemical Name:2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester
CAS No.:79936-79-1
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:199.266
Hs Code.:

Synonyms:2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

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Chemical Property of 2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

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Technology Process of 2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

There total 3 articles about 2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 79936-78-0
(1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

: 2-<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-cyclohexyl>-essigsaure

: 2-<(1'S,2'R)-2'-methyl-6'-methyliden-2'-trideuteriomethyl-cyclohexyl>-essigsauremethylester

: 2-<(6'R)-2',6'-dimethyl-6'-trideuteriomethyl-1'-hexenyl>-essigsauremethylester

: 79936-79-1
2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

Guidance literature:: With lead(IV) acetate; In benzene; at 10 - 15 ℃; for 0.2h; Yield given; Irradiation;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-76-8
C₂₀H₂₅⁽²⁾H₃O₂

: 79936-79-1
2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / 1.17 h / Heating

2: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

3: 16 percent / Pb(OAc)4 / benzene / 0.2 h / 10 - 15 °C / Irradiation

With lead(IV) acetate; hydrogenchloride; potassium permanganate; magnesium sulfate; In acetone; benzene;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-77-9
2-<(1'S,2'S,6'R)-2',6'-dimethyl-2'-(2''-hydroxy-4''-isopropyl)phenyl-6'-triduteriomethyl-cyclohexyl>-essigsauremethylester

: 79936-79-1
2-<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-essigsauremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

2: 16 percent / Pb(OAc)4 / benzene / 0.2 h / 10 - 15 °C / Irradiation

With lead(IV) acetate; potassium permanganate; magnesium sulfate; In acetone; benzene;
DOI:10.1002/hlca.19810640504