Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

Base Information

Chemical Name:Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside
CAS No.:132620-67-8
Molecular Formula:C₁₉H₂₆O₅S
Molecular Weight:366.478
Hs Code.:

Synonyms:Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

Suppliers and Price of Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

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Technology Process of Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

There total 1 articles about Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 23568-31-2
2,3:4,5-di-O-isopropylidene-L-arabinose

: 1822-73-7
phenylthioethylene

: 132620-67-8
Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/S0040-4039(00)74336-X

Reference yield:

: 132620-67-8
Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

: 142405-84-3
Phenyl 3,5-di-O-isopropylidene-2-deoxy-1-thio-α-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

2: 90 percent / p-TsOH*H₂O / acetone / 1.5 h / Ambient temperature

With toluene-4-sulfonic acid; In acetone;
DOI:10.1021/jo00104a020

Reference yield:

: 132620-67-8
Phenyl 3,5:6,7-di-O-isopropylidene-2-deoxy-1-thio-L-gluco-heptofuranoside

: 142405-85-4
Phenyl 3,5-O-benzylidene-2-deoxy-1-thio-α-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

2: 93 percent / p-TsOH*H₂O / CH₂Cl₂ / 1 h / Ambient temperature

With toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1021/jo00104a020