[Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl

Base Information

• Chemical Name: [Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl
• CAS No.: 797790-83-1
• Molecular Formula: C₂₄H₂₇N₄NiO₈S*Cl
• Molecular Weight: 625.709

Synonyms:[Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl

Chemical Property of [Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl

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Technology Process of [Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl

There total 2 articles about [Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H₂O)2]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

nickel(II) chloride hexahydrate + Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) + Piroxicam (36322-90-4) → [Ni(II)(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide 1,1-dioxide)(DL-phenylalaninate)(H2O)2]Cl (797790-83-1)

Guidance literature:

In ethanol; hot EtOH soln. (60°C) of Ni salt added to hot EtOH soln. (60°C) of piroxicam (molar ratio 1:1); phenylalanine (1 equiv.) in EtOH added; stirred under reflux for 30 min; filtered; ppt. washed with hot EtOH and Et2O; dried in vac. desiccator over anhyd. CaCl2; elem. anal.;

DOI:10.1016/j.saa.2004.01.035

Reference yield:

Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) + Piroxicam (36322-90-4) + nickel dichloride (83864-14-6) → [Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H2O)2]Cl (797790-83-1)

Guidance literature:

In ethanol; hot soln. (60°C) of metal salt in EtOH was added to mixt. of hot ethanol soln. (60°C) of piroxicam and soln. of DL-phenylalanine in EtOH in molar ratio 1:1:1; mixt. stirred under reflux for 30 min; ppt. filtered; washed (hot EtOH, Et2O); dried (vac., CaCl2); elem. anal.;

DOI:10.1016/j.saa.2005.06.042

Reference yield:

[Ni(4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide)(DL-phenylalanine)(H2O)2]Cl (797790-83-1) → nickel(II) oxide (1313-99-1)

Guidance literature:

In neat (no solvent); byproducts: H2O, Cl2; heated in dynamic N2 atm. (20 ml/min) with a heating rate of 10°C/min to 870°C; Kinetics;

DOI:10.1016/j.saa.2005.06.042

upstream raw materials:

Phenylalanine

Piroxicam

nickel dichloride

Downstream raw materials:

nickel(II) oxide

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