2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

Base Information

Chemical Name:2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester
CAS No.:204528-05-2
Molecular Formula:C₁₈H₂₂N₄O₅
Molecular Weight:374.396
Hs Code.:

Synonyms:2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

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Chemical Property of 2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

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Technology Process of 2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

There total 2 articles about 2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69195-96-6
5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

: 204528-05-2
2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 1,3-dicyclohexylcarbodiimide / ethyl acetate; dimethylformamide / 1) 0 deg C, 1 h; 2) rt, 1 h

2: 83 percent / dimethylformamide / 3.5 h / 60 °C

3: 71 percent / K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

With potassium carbonate; dicyclohexyl-carbodiimide; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1080/00397919808005949

Reference yield:

: 204527-99-1
1-Benzyl-5-nitro-1H-imidazole-4-carboxylic acid pentafluorophenyl ester

: 204528-05-2
2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / dimethylformamide / 3.5 h / 60 °C

2: 71 percent / K₂CO₃ / dimethylformamide / 3 h / Ambient temperature

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1080/00397919808005949

Reference yield: 78.0%

: 204528-05-2
2-[(1-Benzyl-5-nitro-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

: 204528-06-3
2-[(5-Amino-1-benzyl-1H-imidazole-4-carbonyl)-amino]-hexanoic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 0.75h; under 2068.6 Torr; Ambient temperature;
DOI:10.1080/00397919808005949