meso-phenyl>triphenylporphyrin

Base Information

Chemical Name:meso-phenyl>triphenylporphyrin
CAS No.:80441-45-8
Molecular Formula:C₅₂H₄₃N₅O₂S
Molecular Weight:802.012
Hs Code.:

meso-<o-<6-(acetylthio)hexanamido>phenyl>triphenylporphyrin

Synonyms:meso-phenyl>triphenylporphyrin

Suppliers and Price of meso-phenyl>triphenylporphyrin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-phenyl>triphenylporphyrin

Chemical Property:

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Technology Process of meso-phenyl>triphenylporphyrin

There total 4 articles about meso-phenyl>triphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 69082-94-6
5-(2-aminophenyl)-10,15,20-triphenylporphyrinate

: 80441-58-3
6-(acetylthio)hexanoyl chloride

: 80441-45-8
meso-phenyl>triphenylporphyrin

Guidance literature:: With pyridine; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1021/ja00369a041

Reference yield:

: 502-44-3,24980-41-4,80137-66-2
hexahydro-2H-oxepin-2-one

: 80441-45-8
meso-phenyl>triphenylporphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / conc. HBr, conc. H₂SO₄ / 10 h / Heating

2: K₂CO₃ / H₂O / 12 h / Ambient temperature

3: oxalyl chloride, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

4: 93 percent / pyridine / CH₂Cl₂ / 8 h / Ambient temperature

With pyridine; oxalyl dichloride; sulfuric acid; hydrogen bromide; potassium carbonate; triethylamine; In dichloromethane; water;
DOI:10.1021/ja00369a041

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 80441-45-8
meso-phenyl>triphenylporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / H₂O / 12 h / Ambient temperature

2: oxalyl chloride, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

3: 93 percent / pyridine / CH₂Cl₂ / 8 h / Ambient temperature

With pyridine; oxalyl dichloride; potassium carbonate; triethylamine; In dichloromethane; water;
DOI:10.1021/ja00369a041