3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester

Base Information

• Chemical Name: 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester
• CAS No.: 229487-01-8
• Molecular Formula: C₂₁H₂₄N₂O₇
• Molecular Weight: 416.431

Synonyms:3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester

Chemical Property of 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester

Chemical Property:

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Technology Process of 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester

There total 3 articles about 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester (3160-47-2) + 2-methylaminomethyl-benzene-1,4-diol (229486-97-9) → 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester (229487-01-8)

Guidance literature:

With dicyclohexyl-carbodiimide;

DOI:10.1055/s-1999-3094

Reference yield:

2,5-Dihydroxybenzaldehyde (1194-98-5) → 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester (229487-01-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol; toluene

2: H₂ / 10 percent Pd/C / ethanol

3: 46 percent / DCC

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; toluene;

DOI:10.1055/s-1999-3094

Reference yield:

2-[(E)-Methyliminomethyl]-benzene-1,4-diol → 3-benzyloxycarbonylamino-N-(2,5-dihydroxy-benzyl)-N-methyl-succinamic acid methyl ester (229487-01-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂ / 10 percent Pd/C / ethanol

2: 46 percent / DCC

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol;

DOI:10.1055/s-1999-3094

upstream raw materials:

N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester

2-methylaminomethyl-benzene-1,4-diol

2,5-Dihydroxybenzaldehyde

Downstream raw materials:

(3S)-methyl 3-amino-4-butanoate

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