ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

Base Information

Chemical Name:ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride
CAS No.:1201815-23-7
Molecular Formula:C₉H₁₅NO₂*ClH
Molecular Weight:205.685
Hs Code.:

Synonyms:ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

Suppliers and Price of ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

There total 1 articles about ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-17-5
ethanol

: 193673-65-3,285560-96-5,285560-97-6,473835-79-9,785015-46-5
(1R,2S)-cis-2-aminocyclohex-3-enecarboxylic acid

: 1201815-23-7
ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

Guidance literature:: With thionyl chloride; at -15 ℃; Reflux;
DOI:10.1016/j.tetasy.2009.09.001

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1201815-23-7
ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

: 1201815-24-8
ethyl (1R,2S)-2-(tert-butoxycarbonylamino)cyclohex-3-enecarboxylate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 8h;
DOI:10.1016/j.tet.2011.12.065

Reference yield:

: 1201815-23-7
ethyl (1R,2S)-2-aminocyclohex-3-enecarboxylate hydrochloride

: 1378923-14-8
ethyl (1R,2R,3S,4S)-2-(tert-butoxycarbonylamino)-4-cyano-3-hydroxycyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 8 h / 0 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 0 °C

3: toluene / 15 h / 20 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tet.2011.12.065