methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

Base Information

Chemical Name:methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate
CAS No.:1438868-29-1
Molecular Formula:C₂₅H₂₄O₇S
Molecular Weight:468.527
Hs Code.:

Synonyms:methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

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Chemical Property of methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

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Technology Process of methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

There total 11 articles about methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1438868-20-2
methyl 6-(2-(benzyloxy)-4-(methylthio)-6-(((tetrahydro-2H-pyran-2-yl)oxy)methyl)phenoxy)-3-formyl-2-methoxybenzoate

: 1438868-29-1
methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

Guidance literature:: With toluene-4-sulfonic acid; In water; isopropyl alcohol; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/cjoc.201200977

Reference yield:

: C₁₇H₁₈O₃S

: 1438868-29-1
methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-dimethyl-formamide / 25 °C / Inert atmosphere

2.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

3.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux

With hydrogenchloride; dmap; water; copper; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977

Reference yield:

: C₁₈H₂₀O₃S

: 1438868-29-1
methyl 6-(2-(benzyloxy)-6-(hydroxymethyl)-4-(methylthio)phenoxy)-3-formyl-2-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; hydrogenchloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

2.1: toluene-4-sulfonic acid / dichloromethane / 0.25 h / -10 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

3.1: copper; copper(II) oxide; dmap / acetonitrile / Inert atmosphere; Reflux

4.1: toluene-4-sulfonic acid / water; isopropyl alcohol / 12 h / Inert atmosphere; Reflux

With hydrogenchloride; dmap; water; copper; toluene-4-sulfonic acid; copper(II) oxide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1002/cjoc.201200977