9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

Base Information

Chemical Name:9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole
CAS No.:1350752-94-1
Molecular Formula:C₅₄H₃₈N₂O₂P₂
Molecular Weight:808.855
Hs Code.:

Synonyms:9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

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Chemical Property of 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

Chemical Property:

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Technology Process of 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

There total 5 articles about 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphino)-9H-carbazole

: 1350752-94-1
9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

Guidance literature:: With dihydrogen peroxide; In dichloromethane; at 20 ℃;
DOI:10.1039/c2jm30742a

Reference yield:

: 185112-61-2
9-(3-bromophenyl)carbazole

: 1350752-94-1
9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: dibenzo-18-crown-6; copper; potassium carbonate / 1,2-dichloro-benzene / 12 h / 100 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: dihydrogen peroxide / dichloromethane / 20 °C

With dibenzo-18-crown-6; n-butyllithium; dihydrogen peroxide; copper; potassium carbonate; In tetrahydrofuran; hexane; dichloromethane; 1,2-dichloro-benzene; 1.1: Ullmann reaction;
DOI:10.1039/c2jm30742a

Reference yield:

: 1353645-94-9
9-(3-(9H-carbazole-9-yl)phenyl)-3,6-dibromo-9H-carbazole

: 1350752-94-1
9-(3-(9H-carbazole-9-yl)phenyl)-3,6-bis(diphenylphosphoryl)-9H-carbazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dihydrogen peroxide / dichloromethane / 20 °C

With n-butyllithium; dihydrogen peroxide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c2jm30742a