(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1351458-42-8
Molecular Formula:C₁₅H₂₀BIO₂
Molecular Weight:370.038
Hs Code.:

Synonyms:(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

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Technology Process of (Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about (Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: C₉H₁₀BIO₂

: 1351458-42-8
(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: In tetrahydrofuran; at 23 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100420

Reference yield: 83.0%

: 1351458-42-8
(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 591-51-5
phenyllithium

: 1351458-51-9
(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: phenyllithium; With zinc dibromide; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 23 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100420

Reference yield:

: 1351458-42-8
(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1351458-59-7
(E)-hept-2-ene-1,3-diyldibenzene

Guidance literature:: Multi-step reaction with 2 steps

1: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 23 °C / Inert atmosphere

2: dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere; Reflux

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(ll); tetrabutyl ammonium fluoride; In tetrahydrofuran; 1: Negishi coupling reaction / 2: Suzuki coupling;
DOI:10.1002/adsc.201100420