(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1351458-51-9
Molecular Formula:C₂₁H₂₅BO₂
Molecular Weight:320.239
Hs Code.:

Synonyms:(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 6 articles about (Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1351458-42-8
(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 591-51-5
phenyllithium

: 1351458-51-9
(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: phenyllithium; With zinc dibromide; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

(Z)-2-(1-iodo-3-phenylprop-1-enyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 23 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100420

Reference yield:

: C₂₂H₂₂N₂O₂S

: 73183-34-3
bis(pinacol)diborane

: (E)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1351458-51-9
(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With 2,5-Dimethyl-1,4-benzoquinone; palladium diacetate; sodium hydride; triphenylphosphine; In toluene; at 90 ℃; for 10h; Overall yield = 71 percent; Overall yield = 68.3 mg; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.1c02331

Reference yield:

: 1083-30-3
dihydrochalcone

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 73183-34-3
bis(pinacol)diborane

: (E)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1351458-51-9
(Z)-2-(1,3-diphenylprop-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: dihydrochalcone; toluene-4-sulfonic acid hydrazide; In methanol; at 70 ℃; for 2h; Inert atmosphere; Schlenk technique;

bis(pinacol)diborane; With 2,5-Dimethyl-1,4-benzoquinone; palladium diacetate; sodium hydride; triphenylphosphine; In toluene; at 90 ℃; for 10h; Overall yield = 62 percent; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.1c02331