N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

Base Information

Chemical Name:N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate
CAS No.:131058-14-5
Molecular Formula:C₃₇H₃₉N₅O₁₂S
Molecular Weight:777.809
Hs Code.:

Synonyms:N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

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Chemical Property of N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

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Technology Process of N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

There total 8 articles about N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 131058-13-4
N-<4-(7-amino-10H-indolo<3,2-b>quinolin-11-yl)amino-3-methoxyphenyl>methanesulfonamide

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 131058-14-5
N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1248/cpb.40.1481

Reference yield:

: 80271-19-8
11-chloro-10H-indolo-[3,2-b]quinoline

: 131058-14-5
N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / conc. nitric acid / acetic acid / 10 h / Ambient temperature

2: 67 percent / 2-ethoxy-ethanol / 8 h / Heating

3: 72 percent / H₂ / 10percent Pd/C / acetic acid / 48 h / 760 Torr

4: 30 percent / pyridine / dimethylformamide / 24 h / Ambient temperature

With pyridine; hydrogen; nitric acid; palladium on activated charcoal; In 2-ethoxy-ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.1481

Reference yield:

: 131058-48-5
11-chloro-7-nitro-10H-indolo<3,2-b>quinoline

: 131058-14-5
N-<4-<7-(glucopyranosyl)amino-10H-indolo<3,2-b>quinolin-11-yl>amino-3-methoxyphenyl>methanesulfonamide 2,3,4,6-O-tetraacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / 2-ethoxy-ethanol / 8 h / Heating

2: 72 percent / H₂ / 10percent Pd/C / acetic acid / 48 h / 760 Torr

3: 30 percent / pyridine / dimethylformamide / 24 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In 2-ethoxy-ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.1481