Technology Process of C25H22N2O5
There total 6 articles about C25H22N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
[bis(acetoxy)iodo]benzene; trifluoroacetic acid;
In
methanol;
at 20 - 25 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol; water / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C
4: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 3 h / 0 °C
5: potassium carbonate / methanol / 2 h / 20 - 25 °C
6: [bis(acetoxy)iodo]benzene; trifluoroacetic acid / methanol / 20 - 25 °C
With
[bis(acetoxy)iodo]benzene; hydroxylamine hydrochloride; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide / methanol; water / Reflux
2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C
3: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C
4: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 3 h / 0 °C
5: potassium carbonate / methanol / 2 h / 20 - 25 °C
6: [bis(acetoxy)iodo]benzene; trifluoroacetic acid / methanol / 20 - 25 °C
With
[bis(acetoxy)iodo]benzene; hydroxylamine hydrochloride; sodium acetate; sulfur trioxide pyridine complex; potassium carbonate; dimethyl sulfoxide; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;