methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Base Information

• Chemical Name: methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate
• CAS No.: 1209012-78-1
• Molecular Formula: C₃₂H₃₅ClF₂N₂O₁₂
• Molecular Weight: 713.086

Synonyms:methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property of methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

Chemical Property:

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Technology Process of methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

There total 1 articles about methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-azido-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)-onate (1209012-72-5) + 4-chloro-benzoyl chloride (122-01-0) → methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209012-78-1)

Guidance literature:

With triphenylphosphine; In 1,2-dichloro-ethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jm901517k

Reference yield: 64.0%

methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209012-78-1) → sodium (2,3-difluorobenzyl 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209012-84-9)

Guidance literature:

With water; sodium hydroxide; In methanol; at 20 ℃; for 3h;

DOI:10.1021/jm901517k

Reference yield: 61.0%

methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate (1209012-78-1) → methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid]onate (1241906-46-6)

Guidance literature:

With sodium methylate; In methanol; for 2h;

DOI:10.1016/j.carres.2010.03.010

upstream raw materials:

methyl (2,3-difluorobenzyl 5-acetamido-4,7,8-tri-O-acetyl-9-azido-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)-onate

4-chloro-benzoyl chloride

Downstream raw materials:

sodium (2,3-difluorobenzyl 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate

methyl [(2,3-difluorobenzyl) 5-acetamido-9-(4-chlorobenzamido)-3,5,9-trideoxy-D-glycero-α-D-galacto-2-nonulopyranosid]onate

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