Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl-

Base Information

Chemical Name:Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl-
CAS No.:166330-12-7
Molecular Formula:C38H30 O P2 S
Molecular Weight:596.669
Hs Code.:

Synonyms:Phosphine,(2,8-dimethyl-4,6-phenoxathiindiyl)bis[diphenyl- (9CI); Thixantphos

Suppliers and Price of Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl-

There total 1 articles about Phosphine,1,1'-(2,8-dimethyl-4,6-phenoxathiindiyl)bis[1,1-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-58-3
phenylmagnesium bromide

: 216667-41-3
4,5-bis(dichlorophosphino)-2,7-dimethylphenoxathiin

: 166330-12-7
4,6-bis(diphenylphosphanyl)-2,8-dimethylphenoxathiine

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1021/ja981969e

Reference yield: 99.0%

: nickel(II) chloride hexahydrate

: 166330-12-7
4,6-bis(diphenylphosphanyl)-2,8-dimethylphenoxathiine

: 214049-97-5
[NiCl₂(C₃₈H₃₀OP₂S)]

Guidance literature:: In benzene; (argon); 323 K, 3 h; elem. anal.;
DOI:10.1039/a802269k

Reference yield: 91.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 166330-12-7
4,6-bis(diphenylphosphanyl)-2,8-dimethylphenoxathiine

: 205319-09-1
Pd(C₃₈H₃₀P₂OS)Cl₂

Guidance literature:: In tetrahydrofuran; N2 atmosphere, stirring (room temp., overnight); removement of solvent (vacuum), washing (Et2O), drying (vacuum);
DOI:10.1002/(SICI)1099-0682(199802)1998:2<155::AID-EJIC155>3.0.CO;2-T