3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

Base Information

Chemical Name:3-cyclohexylmethyl-2-oxobutyl benzenesulfonate
CAS No.:84855-88-9
Molecular Formula:C₁₇H₂₄O₄S
Molecular Weight:324.441
Hs Code.:

Synonyms:3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

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Technology Process of 3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

There total 5 articles about 3-cyclohexylmethyl-2-oxobutyl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 84855-57-2
3-cyclohexylmethyl-1-diazo-2-butanone

: 98-11-3
benzenesulfonic acid

: 84855-88-9
3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

Guidance literature:: DOI:10.1248/cpb.35.2426

Reference yield: 74.8%

: 26158-00-9,5928-72-3
benzene-sulfonic acid monohydrate

: 84855-57-2
3-cyclohexylmethyl-1-diazo-2-butanone

: 84855-88-9
3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

Guidance literature:

Reference yield:

: 1009-67-2
2-methyl-3-phenylpropanoic acid

: 84855-88-9
3-cyclohexylmethyl-2-oxobutyl benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / H₂ / PtO₂ / acetic acid / 4 h / 38000 Torr / Ambient temperature

2: thionyl chloride / 5 h / Heating

3: diethyl ether / 1 h

4: 75 percent

With thionyl chloride; hydrogen; platinum(IV) oxide; In diethyl ether; acetic acid;
DOI:10.1248/cpb.35.2426