4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

Base Information

Chemical Name:4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin
CAS No.:845790-96-7
Molecular Formula:C₇₆H₉₃N₅O₂₄Si
Molecular Weight:1488.68
Hs Code.:

Synonyms:4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

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Technology Process of 4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

There total 1 articles about 4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 845883-89-8
4',6'-O-benzylidene-penta-N-benzyloxycarbonyl paromomycin

: 69739-34-0
t-butyldimethylsiyl triflate

: 845790-96-7
4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

Guidance literature:: With 2,4,6-trimethyl-pyridine; In dichloromethane; at 0 ℃; for 24h;

Reference yield: 85.0%

: 845790-96-7
4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin

: 622-24-2
2-phenylethyl chloride

: IBI⁽⁵⁶⁰⁾S₀₀₂₈₂

Guidance literature:: 4',6'-O-benzylidene-penta-N-benzyloxycarbonyl-5''-O-tertbutyldiinethylsilyl paromomycin; 2-phenylethyl chloride; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 20 ℃;

With methanol; sodium methylate;

With water; hydrogen; acetic acid; palladium(II) hydroxide/carbon; more than 3 stages;