Technology Process of 4,4'-bis[(biphenyl-4-yl)-(phenyl-d5)-amino]biphenyl
There total 4 articles about 4,4'-bis[(biphenyl-4-yl)-(phenyl-d5)-amino]biphenyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; sodium sulfite;
3,5-ditertbutyl salicylic acid; copper;
In
1-dodecylbenzene;
at 210 ℃;
for 11h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid / 4 h / 70 °C / Inert atmosphere
2: potassium carbonate; sodium sulfite / copper / 1-dodecylbenzene / 34 h / 210 °C / Inert atmosphere
3: potassium hydroxide; water / i-Amyl alcohol / 3 h / Inert atmosphere; Reflux
4: potassium carbonate; sodium sulfite / 3,5-ditertbutyl salicylic acid; copper / 1-dodecylbenzene / 11 h / 210 °C / Inert atmosphere
With
water; potassium carbonate; acetic acid; potassium hydroxide; sodium sulfite;
3,5-ditertbutyl salicylic acid; copper;
In
i-Amyl alcohol; 1-dodecylbenzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; sodium sulfite / copper / 1-dodecylbenzene / 34 h / 210 °C / Inert atmosphere
2: potassium hydroxide; water / i-Amyl alcohol / 3 h / Inert atmosphere; Reflux
3: potassium carbonate; sodium sulfite / 3,5-ditertbutyl salicylic acid; copper / 1-dodecylbenzene / 11 h / 210 °C / Inert atmosphere
With
water; potassium carbonate; potassium hydroxide; sodium sulfite;
3,5-ditertbutyl salicylic acid; copper;
In
i-Amyl alcohol; 1-dodecylbenzene;
