2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol

Base Information

• Chemical Name: 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol
• CAS No.: 1291070-40-0
• Molecular Formula: C₂₁H₃₀N₂O
• Molecular Weight: 326.482

Synonyms:2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol

Chemical Property of 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol

Chemical Property:

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Technology Process of 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol

There total 1 articles about 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-(adamantan-1-yl)-2-hydroxy-5-methylbenzaldehyde (231963-91-0) + N-methyl-ethane-1,2-diamine (109-81-9) → 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol (1291070-40-0)

Guidance literature:

In benzene; for 2h; Reflux;

DOI:10.1002/anie.201007678

Reference yield: 100.0%

2-(bromomethyl)-4,6-diiodophenol (1210052-81-5) + 2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol (1291070-40-0) → HOC6H2I2CH2N(Me)C2H4NCHC6H2(OH)(Me)(adamantyl) (1291070-43-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 2h;

DOI:10.1002/anie.201007678

Reference yield: 100.0%

2-[(2-(methylamino)ethylimino)methyl]-4-methyl-6-(adamantan-1-yl)phenol (1291070-40-0) + 3,5-di-tert-butyl-2-hydroxybenzyl bromide (194734-57-1) → C36H52N2O2 (1352911-78-4)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 2h;

upstream raw materials:

3-(adamantan-1-yl)-2-hydroxy-5-methylbenzaldehyde

N-methyl-ethane-1,2-diamine

Downstream raw materials:

HOC₆H₂I₂CH₂N(Me)C₂H₄NCHC₆H₂(OH)(Me)(adamantyl)

C₂₉H₃₇ClN₂O₂

C₃₆H₅₂N₂O₂

C₂₈H₃₄Cl₂N₂O₂

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