4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Base Information

Chemical Name:4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol
CAS No.:1516888-22-4
Molecular Formula:C₁₆H₁₀BrN₇O₂S
Molecular Weight:444.271
Hs Code.:

Synonyms:4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Suppliers and Price of 4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

There total 4 articles about 4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1516887-94-7
4-amino-5-(6-bromoimidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

: 555-16-8
4-nitrobenzaldehdye

: 1516888-22-4
4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Guidance literature:: With sulfuric acid; In ethanol; at 80 ℃;
DOI:10.1007/s00044-013-0887-7

Reference yield:

: 1072-97-5
5-bromo-2-pyridylamine

: 1516888-22-4
4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 4 steps

1.1: ethanol / 6 h / 80 °C

2.1: hydrazine hydrate / ethanol / 6 h / 80 °C

3.1: potassium hydroxide / ethanol / 8 h / 25 °C

3.2: 6 h / 80 °C

4.1: sulfuric acid / ethanol / 80 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1007/s00044-013-0887-7

Reference yield:

: 67625-37-0
ethyl 6-bromoimidazo<1,2-a>pyridine-2-carboxylate

: 1516888-22-4
4-(4-nitrobenzylideneamino)-5-(6-bromo-imidazo[1,2-a]pyridin-2-yl)-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / ethanol / 6 h / 80 °C

2.1: potassium hydroxide / ethanol / 8 h / 25 °C

2.2: 6 h / 80 °C

3.1: sulfuric acid / ethanol / 80 °C

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1007/s00044-013-0887-7