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C56H82O10Si2

Base Information
  • Chemical Name:C56H82O10Si2
  • CAS No.:1385034-02-5
  • Molecular Formula:C56H82O10Si2
  • Molecular Weight:971.432
  • Hs Code.:
C<sub>56</sub>H<sub>82</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C56H82O10Si2

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Chemical Property of C56H82O10Si2
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Technology Process of C56H82O10Si2

There total 6 articles about C56H82O10Si2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 22 ℃; for 3h;
DOI:10.1021/ol3015682
Guidance literature:
Multi-step reaction with 4 steps
1.1: 2,6-di-tert-butyl-4-methylpyridine; (4R,5R)-2-bromo-1,3-bis[(4-methylphenyl)sulfonyl]-4,5-diphenyl-1,3,2-diazaborolidine / dichloromethane / 16 h / 0 - 22 °C / Inert atmosphere
1.2: 2 h / -78 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 22 °C / Inert atmosphere
3.1: magnesium bromide ethyl etherate / dichloromethane / 0.08 h / -78 °C / Inert atmosphere
3.2: 12 h / -26 °C / Inert atmosphere
4.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h / 22 °C
With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; 2,6-di-tert-butyl-4-methylpyridine; (4R,5R)-2-bromo-1,3-bis[(4-methylphenyl)sulfonyl]-4,5-diphenyl-1,3,2-diazaborolidine; magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol3015682
Guidance literature:
Multi-step reaction with 6 steps
1.1: 1H-imidazole / dichloromethane
2.1: methylenedimethyl sulfurane / tetrahydrofuran / -10 °C
3.1: 2,6-di-tert-butyl-4-methylpyridine; (4R,5R)-2-bromo-1,3-bis[(4-methylphenyl)sulfonyl]-4,5-diphenyl-1,3,2-diazaborolidine / dichloromethane / 16 h / 0 - 22 °C / Inert atmosphere
3.2: 2 h / -78 °C / Inert atmosphere
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 22 °C / Inert atmosphere
5.1: magnesium bromide ethyl etherate / dichloromethane / 0.08 h / -78 °C / Inert atmosphere
5.2: 12 h / -26 °C / Inert atmosphere
6.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h / 22 °C
With 1H-imidazole; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; 2,6-di-tert-butyl-4-methylpyridine; methylenedimethyl sulfurane; (4R,5R)-2-bromo-1,3-bis[(4-methylphenyl)sulfonyl]-4,5-diphenyl-1,3,2-diazaborolidine; magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol3015682
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