Technology Process of C41H55N7O7Si
There total 16 articles about C41H55N7O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide;
at 55 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: isopropyl alcohol / 3 h / 90 °C
2: iron; acetic acid / 2 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide; 1,2-dichloro-ethane / 2 h / 55 °C
With
iron; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,2-dichloro-ethane; N,N-dimethyl-formamide; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 32 h / 70 - 100 °C / Sealed tube
1.2: 16 h / 100 °C / Sealed tube
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 65 °C / Sealed tube
3.1: lithium hydroxide monohydrate / water; tetrahydrofuran / 2 h / 65 °C / Sealed tube
4.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide; 1,2-dichloro-ethane / 2 h / 55 °C
With
pyridine; lithium hydroxide monohydrate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;