C₃₆H₄₂ClN₇O₇

Base Information

Chemical Name:C₃₆H₄₂ClN₇O₇
CAS No.:1312610-72-2
Molecular Formula:C₃₆H₄₂ClN₇O₇
Molecular Weight:720.225
Hs Code.:

C<sub>36</sub>H<sub>42</sub>ClN<sub>7</sub>O<sub>7</sub>

Synonyms:C₃₆H₄₂ClN₇O₇

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Chemical Property of C₃₆H₄₂ClN₇O₇

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Technology Process of C₃₆H₄₂ClN₇O₇

There total 10 articles about C₃₆H₄₂ClN₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1312610-71-1
C₃₇H₄₄ClN₇O₇

: 1312610-72-2
C₃₆H₄₂ClN₇O₇

Guidance literature:: C₃₇H₄₄ClN₇O₇; With boron tribromide; In dichloromethane; at -70 - 20 ℃;

With water; In dichloromethane; Cooling with ice;

di-tert-butyl dicarbonate; With sodium hydrogencarbonate; In methanol; at 20 ℃; for 3h; pH=7 - 8;

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-72-2
C₃₆H₄₂ClN₇O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

6.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

6.2: -5 - 20 °C

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

8.1: ammonium acetate / toluene / Reflux

9.1: boron tribromide / dichloromethane / -70 - 20 °C

9.2: Cooling with ice

9.3: 3 h / 20 °C / pH 7 - 8

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; sulfuric acid; ammonium acetate; water; boron tribromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 3.1: Suzuki Coupling;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-72-2
C₃₆H₄₂ClN₇O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

5.1: dichloromethane; diethyl ether / 2 h / -5 - 20 °C

5.2: -5 - 20 °C

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

7.1: ammonium acetate / toluene / Reflux

8.1: boron tribromide / dichloromethane / -70 - 20 °C

8.2: Cooling with ice

8.3: 3 h / 20 °C / pH 7 - 8

With tert.-butylnitrite; oxalyl dichloride; lithium hydroxide monohydrate; ammonium acetate; water; boron tribromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 2.1: Suzuki Coupling;