N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)

Base Information

• Chemical Name: N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)
• CAS No.: 1260074-31-4
• Molecular Formula: C₃₆H₄₂N₈
• Molecular Weight: 586.783

Synonyms:N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)

Chemical Property of N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)

Chemical Property:

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Technology Process of N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine)

There total 3 articles about N₁,N₁'-(1,3-phenylenebis(methylene))bis(N₂,N₂'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C36H38N8 (1227512-79-9) → N1,N1'-(1,3-phenylenebis(methylene))bis(N2,N2'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine) (1260074-31-4)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 12h;

DOI:10.1021/ic501951f

Reference yield:

(2-aminoethyl)bis(2-pyridylmethyl)amine (189440-33-3) → N1,N1'-(1,3-phenylenebis(methylene))bis(N2,N2'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine) (1260074-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 24 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 3 h / Molecular sieve; Inert atmosphere; Reflux

With sodium tetrahydroborate; In methanol;

DOI:10.1039/c0dt00165a

Reference yield:

Isophthalaldehyde (626-19-7) → N1,N1'-(1,3-phenylenebis(methylene))bis(N2,N2'-bis(pyridin-2-ylmethyl)ethan-1,2-diamine) (1260074-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 24 h / Molecular sieve; Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 3 h / Molecular sieve; Inert atmosphere; Reflux

With sodium tetrahydroborate; In methanol;

DOI:10.1039/c0dt00165a

upstream raw materials:

C₃₆H₃₈N₈

Isophthalaldehyde

(2-aminoethyl)bis(2-pyridylmethyl)amine

Downstream raw materials:

diethyl 2,2'-(1,3-phenylenebis(methylene))bis((2-(bis(pyridin-2-ylmethyl)amino)ethyl)azanediyl)diacetate

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