Technology Process of C48H88O4S2Si4
There total 8 articles about C48H88O4S2Si4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
magnesium bromide ethyl etherate;
In
diethyl ether;
at 20 ℃;
for 4h;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 7 steps
1: pyridinium p-toluenesulfonate / tetrahydrofuran / 20 °C
2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane
3: water; acetic acid / 1.5 h / 20 °C
4: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C
5: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C
6: oxalyl dichloride; dimethyl sulfoxide / -78 °C
7: magnesium bromide ethyl etherate / diethyl ether / 4 h / 20 °C
With
2,6-dimethylpyridine; oxalyl dichloride; 20 % Pd(OH)2/C; water; hydrogen; pyridinium p-toluenesulfonate; magnesium bromide ethyl etherate; acetic acid; dimethyl sulfoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1055/s-0030-1260586
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; acetic acid / 1.5 h / 20 °C
2: 2,6-dimethylpyridine / dichloromethane / 2.5 h / -15 - 0 °C
3: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 24 h / 20 °C
4: oxalyl dichloride; dimethyl sulfoxide / -78 °C
5: magnesium bromide ethyl etherate / diethyl ether / 4 h / 20 °C
With
2,6-dimethylpyridine; oxalyl dichloride; 20 % Pd(OH)2/C; water; hydrogen; magnesium bromide ethyl etherate; acetic acid; dimethyl sulfoxide;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1055/s-0030-1260586
