C₃₇H₆₀O₃Si₃

Base Information

Chemical Name:C₃₇H₆₀O₃Si₃
CAS No.:146175-87-3
Molecular Formula:C₃₇H₆₀O₃Si₃
Molecular Weight:637.138
Hs Code.:

C<sub>37</sub>H<sub>60</sub>O<sub>3</sub>Si<sub>3</sub>

Synonyms:C₃₇H₆₀O₃Si₃

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Chemical Property of C₃₇H₆₀O₃Si₃

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Technology Process of C₃₇H₆₀O₃Si₃

There total 22 articles about C₃₇H₆₀O₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₆₁IO₃Si₃

: 146175-87-3
C₃₇H₆₀O₃Si₃

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 80 ℃; Yield given;
DOI:10.1016/0040-4039(93)88021-A

Reference yield:

: 36838-71-8
4-methylene-tetrahydro-pyran

: 146175-87-3
C₃₇H₆₀O₃Si₃

Guidance literature:: Multi-step reaction with 14 steps

1: TiBr₂(OiPr)2, (R)-(+)-1,1'-bi-2-naphthol / CH₂Cl₂ / 240 h / -23 °C

2: 91 percent

3: LiAlH₄

4: pyridine

5: dimethylsulfoxide

6: 79 percent / DIBAL-H

7: 87 percent / MeAl(OMe)Cl / CH₂Cl₂ / -10 to 10 deg C

9: 95 percent / CrO₃, 3,5-dimethylpyrazole

10: 83 percent / NaBH₄, CeCl₃

11: 71 percent / imidazole / dimethylformamide

12: pyridine

13: NaI / dimethylformamide

14: DBU / dimethylformamide / 80 °C

With pyridine; 1H-imidazole; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; diisopropoxytitanium(IV) dibromide; (R)-1,1'-Bi-2-naphthol; (Methyl-methoxy-aluminium)-chlorid; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(93)88021-A

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 146175-87-3
C₃₇H₆₀O₃Si₃

Guidance literature:: Multi-step reaction with 15 steps

1: 75 percent / t-BuOK

2: TiBr₂(OiPr)2, (R)-(+)-1,1'-bi-2-naphthol / CH₂Cl₂ / 240 h / -23 °C

3: 91 percent

4: LiAlH₄

5: pyridine

6: dimethylsulfoxide

7: 79 percent / DIBAL-H

8: 87 percent / MeAl(OMe)Cl / CH₂Cl₂ / -10 to 10 deg C

10: 95 percent / CrO₃, 3,5-dimethylpyrazole

11: 83 percent / NaBH₄, CeCl₃

12: 71 percent / imidazole / dimethylformamide

13: pyridine

14: NaI / dimethylformamide

15: DBU / dimethylformamide / 80 °C

With pyridine; 1H-imidazole; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; diisopropoxytitanium(IV) dibromide; potassium tert-butylate; (R)-1,1'-Bi-2-naphthol; (Methyl-methoxy-aluminium)-chlorid; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(93)88021-A