3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

Base Information

Chemical Name:3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone
CAS No.:361145-75-7
Molecular Formula:C₂₂H₁₇ClN₄OS
Molecular Weight:420.922
Hs Code.:

Synonyms:3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

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Chemical Property of 3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

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Technology Process of 3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

There total 2 articles about 3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 36155-35-8
2-[(4-chlorophenyl)sulfanyl]ethanamine

: 119-67-5
o-carboxybenzaldehyde

: 361145-75-7
3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 24h; Heating;
DOI:10.1021/jo010179b

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 361145-75-7
3-(1H-1,2,3-benzotriazol-1-yl)-2-{2-[(4-chlorophenyl)thio]ethyl}-1-isoindolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / K₂CO₃ / CH₂Cl₂ / 48 h / 20 °C

2: 92 percent / p-TsOH*H₂O / toluene / 24 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In dichloromethane; toluene;
DOI:10.1021/jo010179b