5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

Base Information

Chemical Name:5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid
CAS No.:115104-37-5
Molecular Formula:C₂₃H₂₂ClNO₄S₃
Molecular Weight:508.083
Hs Code.:

Synonyms:5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

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Chemical Property of 5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

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Technology Process of 5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

There total 3 articles about 5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 115104-36-4
3-<<(7-chloro-2-quinolinyl)methyl>thio>benzaldehyde

: 107-96-0
3-mercaptopropionic acid

: 115104-37-5
5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 6h; Heating;
DOI:10.1021/jm00099a011

Reference yield:

: 4965-33-7
2-methyl-7-chloroquinoline

: 115104-37-5
5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / NBS, benzoyl peroxide / CCl₄ / 48 h / Heating; Irradiation

2: potassium carbonate / acetone / 0.25 h / Heating

3: 43 percent / p-TsOH / toluene / 6 h / Heating

With N-Bromosuccinimide; Perbenzoic acid; potassium carbonate; toluene-4-sulfonic acid; In tetrachloromethane; acetone; toluene;
DOI:10.1021/jm00099a011

Reference yield:

: 115104-25-1
2-(Bromomethyl)-7-chloroquinoline

: 115104-37-5
5-<3-<<(7-chloro-2-quinolinyl)methyl>thio>phenyl>4,6-dithianonanedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 0.25 h / Heating

2: 43 percent / p-TsOH / toluene / 6 h / Heating

With potassium carbonate; toluene-4-sulfonic acid; In acetone; toluene;
DOI:10.1021/jm00099a011