p-chlorophenyl-p-methylphenylmethanol acetate

Base Information

• Chemical Name: p-chlorophenyl-p-methylphenylmethanol acetate
• CAS No.: 1438894-52-0
• Molecular Formula: C₁₆H₁₅ClO₂
• Molecular Weight: 274.747
• Mol file: 1438894-52-0.mol

Synonyms:p-chlorophenyl-p-methylphenylmethanol acetate

Chemical Property of p-chlorophenyl-p-methylphenylmethanol acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of p-chlorophenyl-p-methylphenylmethanol acetate

There total 1 articles about p-chlorophenyl-p-methylphenylmethanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-chloro-4-(4-methylbenzyl)benzene (30203-87-3) + acetic acid (64-19-7,77671-22-8) → p-chlorophenyl-p-methylphenylmethanol acetate (1438894-52-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane; at 100 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1002/cssc.201200458

Reference yield: 98.0%

p-chlorophenyl-p-methylphenylmethanol acetate (1438894-52-0) → 4'-methyl-4-chlorobenzophenone (5395-79-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; chlorobenzene; at 130 ℃; for 4h;

upstream raw materials:

1-chloro-4-(4-methylbenzyl)benzene

acetic acid

Downstream raw materials:

4'-methyl-4-chlorobenzophenone

Refernces

• 1、 Yi, Hong,Liu, Qiang,Liu, Jie,Zeng, Ziqi,Yang, Yuhong,Lei, Aiwen. "DDQ-catalyzed oxidative C-O coupling of sp3 C-H bonds with carboxylic acids". . p. 2143 - 2146. Retrieved 2013/01/15.