tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane

Base Information

• Chemical Name: tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane
• CAS No.: 183370-86-7
• Molecular Formula: C₄₁H₂₄Cl₂₀O₁₂
• Molecular Weight: 1417.69
• Mol file: 183370-86-7.mol

Synonyms:tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane

Chemical Property of tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane

There total 5 articles about tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(4-carboxy-2-oxabutyl)methane (35638-19-8) → tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane (183370-86-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / 40 °C

2: Et₃N / CHCl₃

With thionyl chloride; triethylamine; In chloroform;

DOI:10.1021/ja9610646

Reference yield:

Pentachlorophenol (87-86-5,67471-28-7) + tetrakis[(carboxyethoxy)methyl]methane tetrachloride (132491-88-4) → tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane (183370-86-7)

Guidance literature:

With triethylamine; In chloroform; Yield given;

DOI:10.1021/ja9610646

Reference yield:

Pentaerythritol (115-77-5) → tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane (183370-86-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 94 percent / 30percent aq. NaOH / Ambient temperature

2: 75 percent / aq. HCl / 4 h / 95 °C

3: SOCl₂ / 40 °C

4: Et₃N / CHCl₃

With hydrogenchloride; sodium hydroxide; thionyl chloride; triethylamine; In chloroform;

DOI:10.1021/ja9610646

upstream raw materials:

Pentachlorophenol

tetrakis[(carboxyethoxy)methyl]methane tetrachloride

Pentaerythritol

tetrakis-[(2-cyanoethoxy)methyl]methane

Downstream raw materials:

2-(6-Methoxy-3-oxo-3H-xanthen-9-yl)-5-[(4-{3-[3-(2-pentachlorophenyloxycarbonyl-ethoxy)-2,2-bis-(2-pentachlorophenyloxycarbonyl-ethoxymethyl)-propoxy]-propionyl}-piperazine-1-carbothioyl)-amino]-benzoic acid methyl ester

C₄₂H₃₉Cl₁₅N₂O₁₃