3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL

Base Information

• Chemical Name: 3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL
• CAS No.: 132491-88-4
• Molecular Formula: C17H24Cl4O8
• Molecular Weight: 498.185
• Mol file: 132491-88-4.mol

Synonyms:TETRAACID CHLORIDE;3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL;3,3'-(2,2-bis((3-chloro-3-oxopropoxy)methyl)propane-1,3-diyl)bis(oxy)dipropanoyl chloride

Chemical Property of 3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL

Chemical Property:

• PSA: 105.20000
• LogP: 2.66120

Purity/Quality:

98% ^*data from raw suppliers

3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL

There total 3 articles about 3,3'-(2,2-BIS((3-CHLORO-3-OXOPROPOXY)METHYL)PROPANE-1,3-DIYL)BIS(OXY)DIPROPANOYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tetrakis(4-carboxy-2-oxabutyl)methane (35638-19-8) → tetrakis[(carboxyethoxy)methyl]methane tetrachloride (132491-88-4)

Guidance literature:

With thionyl chloride; In dichloromethane;

DOI:10.1016/S0957-4166(00)86135-2

Reference yield:

Pentaerythritol (115-77-5) → tetrakis[(carboxyethoxy)methyl]methane tetrachloride (132491-88-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 18 percent / aq. KOH / dioxane / 48 h / 20 °C

2: 31 percent / aq. HCl / 5 h / 70 °C

3: SOCl₂ / 3 h / Heating

With hydrogenchloride; potassium hydroxide; thionyl chloride; In 1,4-dioxane;

DOI:10.1039/b317109d

Reference yield:

tetrakis-[(2-cyanoethoxy)methyl]methane (2465-91-0) → tetrakis[(carboxyethoxy)methyl]methane tetrachloride (132491-88-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 31 percent / aq. HCl / 5 h / 70 °C

2: SOCl₂ / 3 h / Heating

With hydrogenchloride; thionyl chloride;

DOI:10.1039/b317109d

upstream raw materials:

tetrakis(4-carboxy-2-oxabutyl)methane

Pentaerythritol

tetrakis-[(2-cyanoethoxy)methyl]methane

Downstream raw materials:

tetra(2-pentachloro-phenoxycarbonyl-ethoxymethyl)methane

C₄₂H₃₉Cl₁₅N₂O₁₃

Refernces

• 1、 Oh, Nam-Keun,Zin, Wang-Cheol,Im, Jun-Hwan,Ryu, Ja-Hyoung,Lee, Myongsoo. "Organization of branched rod-coil molecules into a 3-D tetragonally perforated lamellar mesophase". . p. 1092 - 1093. Retrieved 2004.
• 2、 -. "Antibodies that inhibit metalloproteins". Page/Page column 29; 30. . Retrieved 2016/01/09.