C₂₂H₂₆FNO₅S

Base Information

Chemical Name:C₂₂H₂₆FNO₅S
CAS No.:1193512-77-4
Molecular Formula:C₂₂H₂₆FNO₅S
Molecular Weight:435.517
Hs Code.:

C<sub>22</sub>H<sub>26</sub>FNO<sub>5</sub>S

Synonyms:C₂₂H₂₆FNO₅S

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Chemical Property of C₂₂H₂₆FNO₅S

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Technology Process of C₂₂H₂₆FNO₅S

There total 10 articles about C₂₂H₂₆FNO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1193512-76-3
C₂₂H₂₈FNO₅S

: 1193512-77-4
C₂₂H₂₆FNO₅S

Guidance literature:: With sodium hypochlorite; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; sodium hydrogencarbonate; sodium bromide; In dichloromethane; water; for 2h;

Reference yield:

: 121-90-4
m-nitrobenzoic acid chloride

: 1193512-77-4
C₂₂H₂₆FNO₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / 16 h / 20 °C / Reflux

2.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux

2.2: 12 h

2.3: 1.5 h

3.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C

4.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C

4.2: 1 h

5.1: sodium hydrogencarbonate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; sodium hypochlorite; sodium bromide / dichloromethane; water / 2 h

With triethylsilane; aluminum (III) chloride; sodium hypochlorite; boron trifluoride diethyl etherate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; tetrabutylammomium bromide; sodium hydrogencarbonate; potassium carbonate; sodium bromide; In ethanol; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 1193512-72-9
1,4-difluoro-3'-nitrobenzophenone

: 1193512-77-4
C₂₂H₂₆FNO₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux

1.2: 12 h

1.3: 1.5 h

2.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C

3.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C

3.2: 1 h

4.1: sodium hydrogencarbonate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; sodium hypochlorite; sodium bromide / dichloromethane; water / 2 h

With triethylsilane; sodium hypochlorite; boron trifluoride diethyl etherate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; tetrabutylammomium bromide; sodium hydrogencarbonate; potassium carbonate; sodium bromide; In ethanol; dichloromethane; water; toluene; acetonitrile;