Technology Process of 1-acetoxyl-3,4-didodecyloxybenzene
There total 4 articles about 1-acetoxyl-3,4-didodecyloxybenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 48.5h;
Inert atmosphere;
Darkness;
DOI:10.1021/ma902460c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride / dichloromethane / 0.17 h / -5 °C / Inert atmosphere
1.2: 2.5 h / -5 - 0 °C / Inert atmosphere; Reflux
2.1: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / dichloromethane / 48.5 h / 0 - 20 °C / Inert atmosphere; Darkness
With
aluminum (III) chloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane;
1.1: Friedel Crafts acylation / 1.2: Friedel Crafts acylation / 2.1: Baeyer-Villiger oxidation;
DOI:10.1021/ma902460c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; potassium iodide / butanone / 16 h / Inert atmosphere; Reflux
2.1: aluminum (III) chloride / dichloromethane / 0.17 h / -5 °C / Inert atmosphere
2.2: 2.5 h / -5 - 0 °C / Inert atmosphere; Reflux
3.1: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / dichloromethane / 48.5 h / 0 - 20 °C / Inert atmosphere; Darkness
With
aluminum (III) chloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; potassium iodide;
In
dichloromethane; butanone;
2.1: Friedel Crafts acylation / 2.2: Friedel Crafts acylation / 3.1: Baeyer-Villiger oxidation;
DOI:10.1021/ma902460c
