4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Base Information

Chemical Name:4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole
CAS No.:1430730-42-9
Molecular Formula:C₄₉H₃₈N₄O₁₁
Molecular Weight:858.861
Hs Code.:

Synonyms:4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

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Chemical Property of 4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

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Technology Process of 4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

There total 5 articles about 4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 706784-62-5
5-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)tetrazole

: 3712-57-0
N-benzyl-4-nitrobenzimidoyl chloride

: 1430730-42-9
4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: In toluene; for 16h; Reflux;
DOI:10.1016/j.ejmech.2014.02.041

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1430730-42-9
4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: calcium chloride; triethylamine / 2 h / 0 - 20 °C

2: thionyl chloride / 2 h / Reflux

3: toluene / 16 h / Reflux

With thionyl chloride; triethylamine; calcium chloride; In toluene;
DOI:10.1016/j.ejmech.2014.02.041

Reference yield:

: 100-46-9
benzylamine

: 1430730-42-9
4-benzyl-5-(4-nitrophenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: calcium chloride; triethylamine / 2 h / 0 - 20 °C

2: thionyl chloride / 2 h / Reflux

3: toluene / 16 h / Reflux

With thionyl chloride; triethylamine; calcium chloride; In toluene;
DOI:10.1016/j.ejmech.2014.02.041