2-Acetoxy-cinnamoylchlorid

Base Information Edit

Chemical Name:2-Acetoxy-cinnamoylchlorid
CAS No.:20996-40-1
Molecular Formula:C₁₁H₉ClO₃
Molecular Weight:224.644
Hs Code.:
Mol file:20996-40-1.mol

Synonyms:2-Acetoxy-cinnamoylchlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Acetoxy-cinnamoylchlorid Edit

Chemical Property:

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Technology Process of 2-Acetoxy-cinnamoylchlorid

There total 4 articles about 2-Acetoxy-cinnamoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 16189-10-9
(E)-3-<2-(acetyloxy)phenyl>-2-propenoic acid

: 20996-40-1
(E)‐2‐(3‐chloro‐3‐oxoprop‐1‐en‐1‐yl)phenyl acetate

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jacs.0c10832

Reference yield:

: 614-60-8
o-Coumaric acid

: 20996-40-1
(E)‐2‐(3‐chloro‐3‐oxoprop‐1‐en‐1‐yl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 0 °C

2: phosphorus pentachloride / dichloromethane / Reflux

With phosphorus pentachloride; sulfuric acid; In dichloromethane;
DOI:10.1016/j.bmc.2017.08.015