C₁₃H₁₄ClFO₂

Base Information

Chemical Name:C₁₃H₁₄ClFO₂
CAS No.:1541198-15-5
Molecular Formula:C₁₃H₁₄ClFO₂
Molecular Weight:256.704
Hs Code.:

C<sub>13</sub>H<sub>14</sub>ClFO<sub>2</sub>

Synonyms:C₁₃H₁₄ClFO₂

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Chemical Property of C₁₃H₁₄ClFO₂

Chemical Property:

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Technology Process of C₁₃H₁₄ClFO₂

There total 6 articles about C₁₃H₁₄ClFO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541198-14-4
C₁₅H₁₈ClFO₃

: 1541198-15-5
C₁₃H₁₄ClFO₂

Guidance literature:: With toluene-4-sulfonic acid; In acetone; at 20 ℃; Inert atmosphere;

Reference yield:

: 14862-52-3
1,3-dibromo-5-chlorobenzene

: 1541198-15-5
C₁₃H₁₄ClFO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / hexane; di-isopropyl ether / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

3.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.08 h / 0 - 25 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 25 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -60 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; hexane; dichloromethane; di-isopropyl ether; acetone; toluene;

Reference yield:

: 188813-05-0
3-bromo-5-chloro-benzaldehyde

: 1541198-15-5
C₁₃H₁₄ClFO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Dean-Stark

2.1: n-butyllithium; N-cyclohexyl-cyclohexanamine / hexane; toluene / 0.08 h / 0 - 25 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 25 °C

4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -60 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / acetone / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; diethylamino-sulfur trifluoride; toluene-4-sulfonic acid; N-cyclohexyl-cyclohexanamine; In tetrahydrofuran; hexane; dichloromethane; acetone; toluene;