2,2-dicyclohexyl-1-butylidenehydrazine

Base Information

• Chemical Name: 2,2-dicyclohexyl-1-butylidenehydrazine
• CAS No.: 935753-45-0
• Molecular Formula: C₁₆H₃₀N₂
• Molecular Weight: 250.428
• Mol file: 935753-45-0.mol

Synonyms:2,2-dicyclohexyl-1-butylidenehydrazine

Chemical Property of 2,2-dicyclohexyl-1-butylidenehydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-dicyclohexyl-1-butylidenehydrazine

There total 9 articles about 2,2-dicyclohexyl-1-butylidenehydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

n-butyllithium (109-72-8,29786-93-4) + N-cyclohexyl-cyclohexanamine (101-83-7) → 2,2-dicyclohexyl-1-butylidenehydrazine (935753-45-0)

Guidance literature:

N-cyclohexyl-cyclohexanamine; With n-butyllithium; In hexane;

With nitric oxide; In tetrahydrofuran; for 3h; under 759811 Torr; cooling;

n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1002/poc.1069

Reference yield: 75.0%

n-butyllithium (109-72-8,29786-93-4) + N-nitrosodicyclohexylamine (947-92-2) → 2,2-dicyclohexyl-1-butylidenehydrazine (935753-45-0) + N,N-dicyclohexyl-N'-(1-propylpentyl)hydrazine

Guidance literature:

In tetrahydrofuran; hexane; at 20 ℃; for 2h; Inert atmosphere; Darkness;

DOI:10.1080/00397910902738120

Reference yield: 68.0%

n-butyllithium (109-72-8,29786-93-4) + N-nitrosodicyclohexylamine (947-92-2) + n-pentyl lithium (3525-31-3) → 2,2-dicyclohexyl-1-butylidenehydrazine (935753-45-0) + N,N-dicyclohexyl-N'-(1-propylhexyl)hydrazine

Guidance literature:

n-butyllithium; N-nitrosodicyclohexylamine; In tetrahydrofuran; hexane; at 20 ℃; for 0.0833333h; Inert atmosphere; Darkness;

n-pentyl lithium; In tetrahydrofuran; hexane; at 20 ℃; for 2h; Inert atmosphere; Darkness;

DOI:10.1080/00397910902738120

upstream raw materials:

n-butyllithium

N-cyclohexyl-cyclohexanamine

N-nitrosodicyclohexylamine

propyllithium

Refernces

• 1、 Vazquez, Alvaro J.,Rodriguez, Cristian,Nudelman, N. Sbarbati. "The reaction of nitrosodicyclohexylamine with organolithiums". experimental part. p. 1098 - 1104. Retrieved 2009/10/26.