N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

Base Information

Chemical Name:N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane
CAS No.:156602-37-8
Molecular Formula:C₁₈H₃₅BN₂Si₂
Molecular Weight:346.471
Hs Code.:

Synonyms:N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

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Technology Process of N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

There total 1 articles about N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 156602-29-8
(CH₂)3N(Si(CH₃)3)B(C₆H₅)NH

: 18162-48-6
tert-butyldimethylsilyl chloride

: 156602-37-8
N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; (dry N2); soln. of n-BuLi slowly added at room temp. to soln. of c-N(Si(CH3)3)B(Ph)NHC3H6/TMEDA, stirred for 1 h at room temp. and refluxed for1 h; after cooling to room temp., t-BuMe2SiCl added slowly, stirred for2 d; filtration, solvent removal, distn.; elem. anal.;

Reference yield:

: 156602-37-8
N-(tert-butyldimethylsilyl)-N'-trimethylsilyl-B-phenyl-1,3,2-diazaboracyclohexane

: 873-51-8
phenylborondichloride

: 156602-48-1
N-phenylchloroboryl-N'-(tert-butyldimethylsilyl)-B-phenyl-1,3,2-diazaboracyclohexane

Guidance literature:: In dichloromethane; byproducts: (CH3)3SiCl; (dry N2); soln. of c-N(t-BuMe2Si)B(Ph)N(SiMe3)C3H6 cooled to 0°C; PhBCl2 added slowly, stirred overnight; solvent removal; elem. anal., yield determined by NMR;