C₅₀H₈₀O₈Si₂

Base Information

Chemical Name:C₅₀H₈₀O₈Si₂
CAS No.:1366246-26-5
Molecular Formula:C₅₀H₈₀O₈Si₂
Molecular Weight:865.351
Hs Code.:

C<sub>50</sub>H<sub>80</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₀H₈₀O₈Si₂

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Chemical Property of C₅₀H₈₀O₈Si₂

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Technology Process of C₅₀H₈₀O₈Si₂

There total 20 articles about C₅₀H₈₀O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1366246-50-5
C₅₄H₈₆O₈Si₂

: 1366246-26-5
C₅₀H₈₀O₈Si₂

Guidance literature:: With Mo(N)(OSi(C₆H₅)3)3(C₅H₅N); In toluene; at 110 ℃; for 8h; Inert atmosphere;
DOI:10.1021/jo300225z

Reference yield:

: 1366246-39-0
C₁₅H₂₀O₃

: 1366246-26-5
C₅₀H₈₀O₈Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: quinoline; hydrogen / ethyl acetate / 2 h

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

3.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

3.2: 3 h / -78 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / Inert atmosphere

5.1: lithium borohydride / methanol; dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

6.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

7.1: pyridine; indium; (1S,2R)-2-Amino-1,2-diphenylethanol / tetrahydrofuran; toluene / 0.75 h / -20 °C / Inert atmosphere

7.2: 16 h / Inert atmosphere

8.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

9.1: dichloromethane / 2 h / 110 °C / Inert atmosphere

9.2: 0.33 h / Inert atmosphere

10.1: Mo(N)(OSi(C₆H₅)3)3(C₅H₅N) / toluene / 8 h / 110 °C / Inert atmosphere

With pyridine; quinoline; indium; lithium borohydride; n-butyllithium; (1S,2R)-2-Amino-1,2-diphenylethanol; oxalyl dichloride; Mo(N)(OSi(C₆H₅)3)3(C₅H₅N); di-n-butylboryl trifluoromethanesulfonate; hydrogen; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate; toluene; 2.1: Swern oxidation / 3.1: Evans aldol reaction / 3.2: Evans aldol reaction / 6.1: Swern oxidation / 7.1: Barbier reaction / 7.2: Barbier reaction;
DOI:10.1021/jo300225z

Reference yield:

: 1366246-14-1
(2R,4Z)-6-[(4-methoxyphenyl)methoxy]-2-methylhex-4-en-1-ol

: 1366246-26-5
C₅₀H₈₀O₈Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

2.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

2.2: 3 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / Inert atmosphere

4.1: lithium borohydride / methanol; dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

6.1: pyridine; indium; (1S,2R)-2-Amino-1,2-diphenylethanol / tetrahydrofuran; toluene / 0.75 h / -20 °C / Inert atmosphere

6.2: 16 h / Inert atmosphere

7.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

8.1: dichloromethane / 2 h / 110 °C / Inert atmosphere

8.2: 0.33 h / Inert atmosphere

9.1: Mo(N)(OSi(C₆H₅)3)3(C₅H₅N) / toluene / 8 h / 110 °C / Inert atmosphere

With pyridine; indium; lithium borohydride; n-butyllithium; (1S,2R)-2-Amino-1,2-diphenylethanol; oxalyl dichloride; Mo(N)(OSi(C₆H₅)3)3(C₅H₅N); di-n-butylboryl trifluoromethanesulfonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; 1.1: Swern oxidation / 2.1: Evans aldol reaction / 2.2: Evans aldol reaction / 5.1: Swern oxidation / 6.1: Barbier reaction / 6.2: Barbier reaction;
DOI:10.1021/jo300225z