1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

Base Information

Chemical Name:1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene
CAS No.:1366246-12-9
Molecular Formula:C₃₄H₃₄O₃
Molecular Weight:490.642
Hs Code.:

Synonyms:1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

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Chemical Property of 1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

Chemical Property:

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Technology Process of 1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

There total 4 articles about 1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4039-83-2
3-(4-methoxybenzyloxy)propyne

: 123595-49-3
(2S)-2-methyl-3-(triphenylmethoxy)-propyl 4-methylbenzenesulfonate

: 1366246-12-9
1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

Guidance literature:: 3-(4-methoxybenzyloxy)propyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.5h; Inert atmosphere;

(2S)-2-methyl-3-(triphenylmethoxy)-propyl 4-methylbenzenesulfonate; In tetrahydrofuran; hexane; dimethyl sulfoxide; for 2h; Inert atmosphere;
DOI:10.1021/jo300225z

Reference yield:

: 116021-13-7
(2S)-2-methyl-3-(trityloxy)propionic acid methyl ester

: 1366246-12-9
1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4 h / -40 °C / Inert atmosphere

2.1: pyridine / 5 h / 0 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

With n-butyllithium; diisobutylaluminium hydride; In tetrahydrofuran; pyridine; hexane; dichloromethane;
DOI:10.1021/jo300225z

Reference yield:

: 76-83-5
trityl chloride

: 1366246-12-9
1-methoxy-4-({[(5R)-5-methyl-6-(triphenylmethoxy)hexyl]oxy}methyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 4 h / -40 °C / Inert atmosphere

3.1: pyridine / 5 h / 0 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

4.2: 2 h / Inert atmosphere

With dmap; n-butyllithium; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; pyridine; hexane; dichloromethane;
DOI:10.1021/jo300225z