C₅₂H₈₃N₄O₇Si₂Br

Base Information

Chemical Name:C₅₂H₈₃N₄O₇Si₂Br
CAS No.:943858-37-5
Molecular Formula:C₅₂H₈₃BrN₄O₇Si₂
Molecular Weight:1012.33
Hs Code.:

C<sub>52</sub>H<sub>83</sub>N<sub>4</sub>O<sub>7</sub>Si<sub>2</sub>Br

Synonyms:C₅₂H₈₃N₄O₇Si₂Br

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Chemical Property of C₅₂H₈₃N₄O₇Si₂Br

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Technology Process of C₅₂H₈₃N₄O₇Si₂Br

There total 17 articles about C₅₂H₈₃N₄O₇Si₂Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 943858-26-2
C₃₄H₄₉N₄O₅BrSi

: 117289-84-6
(E)-(2S,6R,8S)-8-{[tert-butyl(dimethyl)silyl]oxy}-2,4,6-trimethylnon-4-enoic acid

: 943858-37-5
C₅₂H₈₃N₄O₇Si₂Br

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; at 0 - 20 ℃; for 24h;
DOI:10.1021/ol070855h

Reference yield:

: 226703-78-2
C₁₇H₂₁NO₄

: 943858-37-5
C₅₂H₈₃N₄O₇Si₂Br

Guidance literature:: Multi-step reaction with 10 steps

1: 93 percent / propionic acid / 1 h / 140 °C

2: 83 percent / LiBH₄ / ethanol; diethyl ether; tetrahydrofuran / 0.33 h / 0 °C

3: 24 mg / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 6 h / Heating

4: 81 percent / pyridine; AcOH; NaH₂PO₃*H₂O / Raney nickel / H₂O / 6 h / 50 °C

5: tetrahydrofuran / 0.5 h / 0 °C

6: triphenylphosphine; diisopropyl azodicarboxylate / diethyl ether / 10 h / 20 °C

7: 7.8 mg / potassium carbonate / ethanol / 5 h / 20 °C

8: 98 percent / Et₃N / CH₂Cl₂ / 3 h / 20 °C

9: 95 percent / aq. lithium hydroxide / tetrahydrofuran; methanol / 6 h / 20 °C

10: 80 percent / DCC; HOBt / 24 h / 0 - 20 °C

With pyridine; lithium hydroxide; lithium borohydride; sodium dihydrogen phosphate; di-isopropyl azodicarboxylate; potassium carbonate; benzotriazol-1-ol; acetic acid; propionic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; nickel; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; 1: Claisen orthoester rearrangement / 3: Mitsunobu reaction / 6: Mitsunobu reaction;
DOI:10.1021/ol070855h

Reference yield:

: 943858-32-0
C₁₃H₂₁NO₂

: 943858-37-5
C₅₂H₈₃N₄O₇Si₂Br

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / pyridine; AcOH; NaH₂PO₃*H₂O / Raney nickel / H₂O / 6 h / 50 °C

2: tetrahydrofuran / 0.5 h / 0 °C

3: triphenylphosphine; diisopropyl azodicarboxylate / diethyl ether / 10 h / 20 °C

4: 7.8 mg / potassium carbonate / ethanol / 5 h / 20 °C

5: 98 percent / Et₃N / CH₂Cl₂ / 3 h / 20 °C

6: 95 percent / aq. lithium hydroxide / tetrahydrofuran; methanol / 6 h / 20 °C

7: 80 percent / DCC; HOBt / 24 h / 0 - 20 °C

With pyridine; lithium hydroxide; sodium dihydrogen phosphate; di-isopropyl azodicarboxylate; potassium carbonate; benzotriazol-1-ol; acetic acid; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; nickel; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; 3: Mitsunobu reaction;
DOI:10.1021/ol070855h