methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

Base Information

Chemical Name:methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate
CAS No.:1431657-49-6
Molecular Formula:C₂₁H₁₇F₅N₄O₄
Molecular Weight:484.382
Hs Code.:

Synonyms:methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

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Chemical Property of methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

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Technology Process of methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

There total 2 articles about methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 2826-30-4
2-(2-nitrobenzylidene)malononitrile

: 104721-32-6
methyl 4,4,5,5,5-pentafluoropent-2-ynoate

: 1431657-49-6
methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

Guidance literature:: In dichloromethane; at 20 ℃; for 8h;
DOI:10.1016/j.tet.2013.03.093

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1431657-49-6
methyl 4-(tert-butylamino)-3,3-dicyano-2-(2-nitrophenyl)-5-(pentafluoroethyl)cyclopenta-1,4-dienecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 5 h / 20 °C

2: dichloromethane / 8 h / 20 °C

With piperidine; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2013.03.093