(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

Base Information

Chemical Name:(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane
CAS No.:1073828-77-9
Molecular Formula:C₄₄H₅₈O₅Si
Molecular Weight:695.027
Hs Code.:

(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

Synonyms:(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

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Chemical Property of (2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

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Technology Process of (2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

There total 2 articles about (2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: potassium trifluoro[(E)-2-methyl-1,4-pentadienyl]borate

: 1073828-73-5
(2S,5S)-5-((1R,2R,3R)-5-bromo-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3-methyl-5-hexenyl)-2-(3-tert-butyldiphenylsilyloxypropyl)oxolane

: 1073828-77-9
(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

Guidance literature:: With palladium diacetate; caesium carbonate; triphenylphosphine; In tetrahydrofuran; water; at 70 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/ol801923y

Reference yield:

: 1073828-91-7
C₁₂H₂₁BO₂

: 1073828-73-5
(2S,5S)-5-((1R,2R,3R)-5-bromo-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3-methyl-5-hexenyl)-2-(3-tert-butyldiphenylsilyloxypropyl)oxolane

: 1073828-77-9
(2S,5S)-2-(3-tert-butyldiphenylsilyloxypropyl)-5-((1R,2R,3R,6E)-1,2-dihydroxy-1,2-O-((RS)-4-methoxyphenylmethylene)-3,9-dimethyl-5-methylene-6,8-decadienyl)oxolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium hydroxide octahydrate; In N,N-dimethyl-formamide; at 70 ℃; Inert atmosphere;
DOI:10.1021/ol801923y