1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

Base Information

Chemical Name:1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane
CAS No.:77773-81-0
Molecular Formula:C₁₆H₂₁N₇O₆
Molecular Weight:407.386
Hs Code.:

Synonyms:1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

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Chemical Property of 1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

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Technology Process of 1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

There total 2 articles about 1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77773-78-5
N-(1-Azido-2,2-dimethoxypropyl)-p-aminobenzoic acid

: 77773-81-0
1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent palladium on carbon / methanol / 18 h / 1292.9 Torr

2: 80 percent / methanol / 4 h / Heating

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00328a042

Reference yield:

: 77773-77-4
4-[(3-Azido-2,2-dimethoxy-propyl)-(2,2,2-trifluoro-acetyl)-amino]-benzoic acid ethyl ester

: 77773-81-0
1-<(2,4-Diamino-5-nitropyrimidin-6-yl)amino>-2,2-dimethoxy-3-<(p-carboxyphenyl)amino>propane

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 1 N NaOH / tetrahydrofuran / 18 h

2: H₂ / 5percent palladium on carbon / methanol / 18 h / 1292.9 Torr

3: 80 percent / methanol / 4 h / Heating

With sodium hydroxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jo00328a042