6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

Base Information

Chemical Name:6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate
CAS No.:754242-04-1
Molecular Formula:C₂₅H₂₉BrO₆S
Molecular Weight:537.472
Hs Code.:

Synonyms:6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

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Chemical Property of 6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

Chemical Property:

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Technology Process of 6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

There total 3 articles about 6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 176594-44-8
6-bromohexyl nitrate

: 179174-79-9
(2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoic acid

: 754242-04-1
6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

: 6-(nitrooxy)hexyl-(2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

: (Z)-4-Acetoxy-3-(4-methanesulfonyl-phenyl)-2-phenyl-but-2-enoic acid 6-[(Z)-4-acetoxy-3-(4-methanesulfonyl-phenyl)-2-phenyl-but-2-enoyloxy]-hexyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 22 ℃;
DOI:10.1021/jo051712g

Reference yield:

: 179174-79-9
(2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoic acid

: 629-03-8
1 ,6-dibromohexane

: 754242-04-1
6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo051712g

Reference yield:

: 754242-11-0
(Z)-4-Acetoxy-3-(4-methylsulfanyl-phenyl)-2-phenyl-but-2-enoic acid

: 754242-04-1
6-bromohexyl (2Z)-4-(acetyloxy)-3-[4-(methylsulfonyl)phenyl]-2-phenylbut-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 89.8 percent / hydrogen peroxide; acetic acid / 40 °C

2: K₂CO₃ / dimethylformamide

With dihydrogen peroxide; potassium carbonate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jo051712g