N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Base Information

Chemical Name:N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide
CAS No.:1349147-38-1
Molecular Formula:C₆₄H₇₄N₂O₂₀
Molecular Weight:1191.29
Hs Code.:

Synonyms:N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Suppliers and Price of N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

There total 3 articles about N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52995-76-3
1-chloro-3,6,9-trioxadecane

: 1349147-38-1
N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 140 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrazine hydrate / butan-1-ol / 20 °C / Inert atmosphere; Heating; Reflux

3.1: 1H-imidazole / 4.5 h / 140 °C / Inert atmosphere

3.2: 1 h / 20 °C

With 1H-imidazole; palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; butan-1-ol;

Reference yield:

: 1203642-92-5
3,4-di-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}aniline

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1349147-38-1
N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Guidance literature:: 3,4-di-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}aniline; perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride; With 1H-imidazole; at 140 ℃; for 4.5h; Inert atmosphere;

With hydrogenchloride; In water; at 20 ℃; for 1h;

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 1349147-38-1
N,N'-bis-(4-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}phenyl)-3,4:9,10-perylene tetracarboxydiimide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; thionyl chloride / toluene / Heating

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 140 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrazine hydrate / butan-1-ol / 20 °C / Inert atmosphere; Heating; Reflux

4.1: 1H-imidazole / 4.5 h / 140 °C / Inert atmosphere

4.2: 1 h / 20 °C

With pyridine; 1H-imidazole; thionyl chloride; palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; toluene; butan-1-ol;