3-methyl-cyclobutanecarboxylic acid amide

Base Information

Chemical Name:3-methyl-cyclobutanecarboxylic acid amide
CAS No.:89530-97-2
Molecular Formula:C₆H₁₁NO
Molecular Weight:113.159
Hs Code.:

Synonyms:3-methyl-cyclobutanecarboxylic acid amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-cyclobutanecarboxylic acid amide

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Technology Process of 3-methyl-cyclobutanecarboxylic acid amide

There total 1 articles about 3-methyl-cyclobutanecarboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15760-35-7
3-methylenecyclobutanecarbonitrile

: 89530-97-2
3-methyl-cyclobutanecarboxylic acid amide

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C

2: aq. NaOH / 16 h / Heating

3: SOCl₂, Py / 55 - 60 °C

4: NH₃ / diethyl ether / -20 °C

With pyridine; sodium hydroxide; thionyl chloride; ammonia; hydrogen; palladium on activated charcoal; In diethyl ether;
DOI:10.1021/jo01025a001