1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

Base Information

Chemical Name:1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester
CAS No.:612527-34-1
Molecular Formula:C₃₉H₂₈Br₂N₆O₄
Molecular Weight:804.497
Hs Code.:

Synonyms:1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

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Chemical Property of 1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

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Technology Process of 1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

There total 2 articles about 1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.9%

: 612527-33-0
8-bromo-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-3-carboxylic acid

: 504-63-2
trimethyleneglycol

: 612527-34-1
1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

Guidance literature:: 8-bromo-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

trimethyleneglycol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.bmc.2008.08.072

Reference yield: 61.9%

: 504-63-2
trimethyleneglycol

: 612527-34-1
1,3-bis(8-bromo-6-phenyl-4H-ibenzo[f]midazo[1,5-a][1,4]diazepine-3-carboxy)propyl diester

Guidance literature:: 8-bromo-6-phenyl-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-3-carboxylic acid; With 1,1'-carbonyldiimidazole; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2h;

trimethyleneglycol; With 1,8-diazabicyclo[5.4.0]undec-7-ene;