5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol

Base Information

• Chemical Name: 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol
• CAS No.: 68070-76-8
• Molecular Formula: C₁₆H₂₁NO₂
• Molecular Weight: 259.348

Synonyms:5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol

Chemical Property of 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol

Chemical Property:

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Technology Process of 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol

There total 3 articles about 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6-one (68070-79-1) → 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol (68070-76-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.5h;

DOI:10.1021/jo01315a001

Reference yield:

Nitrosobenzene (586-96-9) → 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol (68070-76-8)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 4 h / Ambient temperature

2: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

With lithium aluminium tetrahydride; In diethyl ether; dichloromethane;

DOI:10.1021/jo01315a001

Reference yield:

3,4,6,6-tetramethyl cyclohexa 2,4-diene-1-none (14069-95-5) + Nitrosobenzene (586-96-9) → 5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6endo-ol (68070-76-8)

Guidance literature:

Multistep reaction; (i) LiAlH₄, Et₂O, (ii) /BRN= 605688/, CH₂Cl₂;

DOI:10.1021/jo01315a001

upstream raw materials:

5,5,7,8-tetramethyl-3-phenyl-2-oxa-3-aza-bicyclo[2.2.2]oct-7-en-6-one

3,4,6,6-tetramethyl cyclohexa 2,4-diene-1-none

Nitrosobenzene

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