Technology Process of ethyl (R/S)-2--3,3-diethoxypropionate
There total 5 articles about ethyl (R/S)-2--3,3-diethoxypropionate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen; acetic acid;
palladium dihydroxide; pyrographite;
In
ethanol;
for 48h;
under 3000.2 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 64 percent / sodium cyanoborohydride / methanol / 16 h
2: 78 percent / pyridine / CH2Cl2 / 3 h
3: 80 percent / H2, acetic acid / palladium(II) hydroxide/carbon (20percent) / aq. ethanol / 48 h / 3000.2 Torr
With
pyridine; hydrogen; sodium cyanoborohydride; acetic acid;
palladium dihydroxide; pyrographite;
In
methanol; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / pyridine / CH2Cl2 / 3 h
2: 80 percent / H2, acetic acid / palladium(II) hydroxide/carbon (20percent) / aq. ethanol / 48 h / 3000.2 Torr
With
pyridine; hydrogen; acetic acid;
palladium dihydroxide; pyrographite;
In
ethanol; dichloromethane;